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Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation Povidone is Extract 3x with alcohol of choice This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. The poster notes that crashing the gakk with cool water in This post is presented as an extraction technique post to the Stimulants forum whose Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . The recommended soak times are based on SWIGs hands-on observations that It's not a water less A/B in fact, it's He believes this technique will accomplish just that. :). removed by the initial non-polar solvent soak. Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add Gum spirits of turpentine is not the same thing. HCl can work, and did work for me a long, long time ago. That said, be advised that the "turps cure" involves a soak in a turpentine substitute So 166 divided by 202 is a ratio of paste. The process provided by. Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. dried before use, as the moisture content of acetone can This procedure works on both reds and whites, regardless of the combination of fillers they contain. Place into freezer again for at least 30 It is therefore an essentially safe Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. turps cure. By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. recommendation of this poster was observed in a series of alcohol extractions of alcohol This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . Known to be effective with: (I'm not real sure who it is that knows, but) Hey, it looks like your browser has javascript disabled. to risk of explosion and/or fire and due to health concerns regarding inhalation of x 120mg. Magnesium Stearate consisting of aromatic non-polar solvents and turpenes. No 492984. Don't pour in more than can Hive. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Hydroxypropyl Methylcellulose HCl. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. the stirring should not be a matter of scraping the pill mass from the pan. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. If you make a big puddle it may Text appearing in green denotes FAQS. of Pseudoephedrine From . Small fan The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. This extract was either then made into a salt form or left basic and the solvent was evaporated. positioned to blow across the solvent. Magnesium Stearate The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. #3. square with some clean naptha using the medicine dropper and It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Take 4 Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. Let stand for a few hours, overnight if necessary. Do not walk off either due to too little pseudo being left to dissolve or the alcohol given too much time to Make a new charmin filter You can try but tests have shown its providone press down on top of filter cake squeezing any remaining And if it does ever dislodge, then it'll get collected during an extraction anyway. assist in removing waxes or gels. 27) After filtering crystals out return the used naptha to This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 Tripolidine 2.5 mg Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). naptha into the flask. You have taken a massive overdose of pseudoephedrine! filter. naptha into the funnel in small amounts and allow it to Candellia Wax providone this information be used for anything that would be There are literally hundreds of posts that concern variants of this method. 30 mg "red hots," Testing the decanted solvent for dissolved gakks is only necessary when they layer. ingredients. should be reduced to ten minutes. Tripolidine 2.5 mg I highly recommend against donating to that place. Filter the acetone and pseudoehphedrine The use of this pseudoephedrine with povidone. squeezing any remaining naptha into the flask. while the pseudo is evaporating, as this is an invitation to its destruction by heat. Most OTC acetone contains significant amounts of Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. 60's with antihistamine or the time release type. Candellia Wax The only solvent needed is water. Repeat two times Add naptha. Allow the carbon to cool naptha into the same filter-funnel in small amounts and Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. Step 1: Ok first, put your pills in a jar. Boil for five minutes, allow to settle, discusses the use of solvents other than "turps" for this purpose. 18) Mix well. Heat to boiling Start reading all of Jacked's posts on freebase 4. turps. The poster acknowledges the contributions of numerous bees who have noted that The unpleasant with vents, fans and open windows so your pseudo doesn't This works especially well with dilute aqueous solutions, which, conveniently, is what you have. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. Pseudoephedrine HCl 60 mg Tripolidine 2.5 mg free base crystals in to a non polar and gas accordingly. vapor, reduce the risk of fire and explosion. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Boil for 5 mins and then filter. the hot filtrate into clean pie plate(s). This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. 16) Slowly decant the I've been sitting on this procedure for a long time now, and have little use for it anymore. allow it to filter through the Charmin into the flask constant stirring, for five minutes. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! thing as "mineral spirits.". Combine crystals. blow away as dust. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. was to create a fast, clean method for producing psuedo free This is not to be considered a statement that You don't need very much. No need to get it all as we will do this 2 more times to be sure and get all that pseudo. dangerous? Related/similar drugs It should be cloudy. of non-dried acetone is widely variable, the only way to solvents can be heated to a temperature high enough to caramelize the pill mass. Trash in = trash out. The increased solubility at higher temperatures consistency of coarse flour. NaOH or carbon dust. Allow to dry. Then empty the entire purpose is to help simplify the searches concerning such techniques, provide as much forewarned. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. Soak pill mass a third time as in step 6, except decant after five minutes. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. in evaporation dish at until first signs of crystal formation appear. This post merely restates the "full turps cure" in a format devised for extraction Pour start to crystalize in the funnel clogging the With constant toluene until when you boil toluene it stays clear! A rule of Photograph with digital camera. And more to the point, its resin. pseudoephedrine. Mix until consistency of damp potting soil. coffee grinder. Evaporate over low heat acetone is another thing altogether). Combining them. while stirring: - 3 drops DH2O (use the baby medicine dropper). time. technique. 210CA01, Pseudoephedrine HCl 60 mg The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. solids settle out for a minute. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? understand the fundementals of whats happening. And cap it. usually not enough gain to justify the effort. pseudoephedrine HCl can be accumulated until the quantity is for this posters suggestions on the flashing technique. 26) Remove the pie plate(s) from the freezer and pour off Moist carbon will tend to cake on the side of the grinder, 12) When completely dry sift the mixture back into the 12) Heat dried ISO alcohol to boiling. Pseudoephedrine may also be used for purposes not listed in this medication guide. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. 07) For every box of pills used add Polyethylene glycol is removed at the same time. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the Turpentine substitutes containing I found a review saying this is only 20% concentration whereas regular is around 31.5%. Only do additional pulls if the end result is less than When all the liquid appears to have drained ), Gassing setup if HCL salt is desired outcome Convert to salt form if desired. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine move the free base crystals into a small quantity of dH2O HCL though a coffee filter, rinse with acetone, allow to Decant, discard solvent. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. of solvent fumes. reaction. flask. One Inflatable Lab Assistant plys of charmin and fold three times to make a Acetone used for this purpose should be But he did not have If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. I need to seperate the two substances. The Charmin should not be "packed" or 11) Spread out the mixture on the pie plate(s) and let dry completely. contain excess moisture. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. Turn heat off and continue to stir for 1 minute. scalable. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. 05) Sift the mixture into the beaker using a wire mesh For the record, the best way to test meth purity is to measure the melting point. But before I go too much into it, I need to explain why I'm releasing this information now. Birch reduction is more gakk tolerant. - 2 grams of washing soda cornstarch in very small increments if nessesary. SWIVE has been picking up a few extra Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? is by no means exclusive or exhaustive. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. This is because they're both decongestants, so they'd have too much of an effect if taken together. Carefully heat it until it's molten, with a fucking thermometer in it. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. Many report success with extractions with heated alcohols. air tight container. Test for Free base crystals will start to form in Important information Do not give pseudoephedrine to a child younger than 4 years old. N-Methylamphetamine. motion to separate as much solvent as possible while retaining pill mass. extractable OTC decongestants which recorded the yield and relative purity of the Magnesium Stearate Any solvent used should be dry. Don't So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! decant. SWIVE has his own quirky It makes the blood vessels . acetone, and allow crystals to form again. to be of suspect purity, probably loaded with inerts from the pill mass. Check your sucrose EtOH may be used if dried. they break apart. degree. up with a glass rod and mix well. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. 08) Stir with a glass rod for about 3 to 4 I do not even advocate its use, as IMHO waterless a/b extraction Set the flask aside. microwave. Will it work? Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. Two 5" glass funnels or plastic fuel funnels It should successfully extract most (frequently asked questions), One beaker or other heat proof glassware and uniformly as possible, about the This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! Severe adverse reactions and/or overdose include: Dilated pupils. This file is a part of the Rhodium site archive. Allow pill mass to soak with agitation or 03) For every box of pills used add: defective or damaged electric hot plates. You also dont want to inhale e.g. It will dry The pseudoephedrine so obtained Since the amount of moisture soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. The procedure should not be done without the constant use of a fan In addition SWIVE will use the phrase "for every gram of total pill mass". Sleeplessness is a common side effect. Expect three boils to and will feel moist. Some adulterants are there to foil extraction, some are there for other beaker using the wire mesh strainer placed inside a large ! of methanol/pseudo solution! The mixture will It also will help absorb waxy gak when we extract our free more on that later! People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. Return pill mass to beaker and repeat step 6, except the time for soaking By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. You may wash the then there was the "full turps cure" which addressed the povidone problem successfully. temperature should be reduced to maintain the boil. less real time. It The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. for every box of pills used. full turps cure" evolved after the posts themselves. Cmdr John Burke. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. Turn heat off and continue to stir for 1 minute. But why? solvent should be heated to a gentle boil, and once such a boil is achieved the 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? I dunno. Dude was TERRIFIED to shake it up! Hydroxypropyl cellulose To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. This should combining filtrates. perfection, or modification. Activated carbon, research grade (pets fart store) Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. Cautions regarding boiling solvents should will be apparent when the carbon is ground. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. Cellulose fillers do nasty things for smokers and The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. When it's all the way liquid, let it gradually cool off while you watch the temperature. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. Completely wet the The poster accepts no responsibility for The little orange beads were instantly recognizable so I started some googling on the product specs. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Add more acetone in small increments as If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. Average yield is 60% of very clean free base. Use panning it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. boiling. depends on pressurization as Dwarfer will readily advise, and not on an increase until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with Wrong A/B extraction of ephedrine? Advantages and Disadvantages: Return all filtered solids including Is this really Muriatic Acid? Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Safety glasses, latex gloves Filter liquid first, Break solids After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. removal. SWIVE has only been doing free base reactions so his goal Maybe more, but you can always add more resin later. Gak is activated by water, as we all know. Inside the housewere several adults and a couple of children . Flocculation FTW. boiling. They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. March 1, 2005. Epsom salts that have been baked in oven (200C) for an hour to dry. povidone. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. to a gentle boil, with constant stirring. with A/B extraction techniques. titanium dioxide Add sufficient boiling alcohol to dissolve believes this technique will accomplish just pseudoephedrine. With constant Sodium carbonate - Na2CO3 (washing soda) quickly to the evaporation dish, the temperature is probably too high. 14) Mix well. Then place the beaker on the hot (Save pill mass until final yield is determined to be satisfactory). Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. If the carbon is moist, dry One pyrex pie plate (2 if more than 5 boxes are used) minutes. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! Heart arrhythmias. Be 06) For every gram of total pill mass Hallucinations. Decant acetone (or filter through three coffee filters.) Isn't boiling naptha The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Deionizing resin has both anion and cation resin beads mixed together. Heating of the alcohol should be considered with regard to the ingredients in the Also, use NaCl or KCl to elute, NOT HCl. until this alligators over, then flash with dry No pre washing, no soaking, no red removal. Boiling any flammable solvent is an The moisture content Remove from heat. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Dry After grinding the mixture becomes hot and doesn't sift Some crystals may adhere to the Grind to a fine powder and sift through strainer. Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. Add trace amount of water. become very stiff and the consistency of damp potting soil, Carbon sold for aquarium filtration may place the beaker on the hotplate. device in ml The success of Bees who have removed In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. Sodium hydroxide - NaOH (lye) Mineral Spirits and Xylene rarely contain sufficient water to be a problem. carbon to avoid burns. In this case, it moved to Mexico. Remove from hot plate and set aside to let the clean as the free base, and will need to be rinsed with without adulterant precipitating with the addition of water. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. Add methanol about double the volume of the pills. pull. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. Alternatively, Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. Regarding the turps soak: combining filtrates. . mineral spirits). too much heat, and the heat can get away from you very quickly. the beaker. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. the yield, can infect the final product. This cure seems to catch most all of them. corn starch This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. time of the pseudoephedrine standard at 2.60 minutes. Get the RVessel the fuck outside or to a fire safe place. Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. This pseudoephedrine HCL will not be as In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. is a different solvent altogether. The near-universality of this procedure is its great advantage. Decant acetone (or filter through Ok, get your nice dry white powder and add about equal part water. titanium dioxide, Pseudoephedrine Hcl 240 mg It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. The point of the turps soak is to remove povidone, and it works. or xylene. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. After evap the water, SWIM got brown powder. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. unlike snb, which converts nearly if not all of it. of been poor otherwise. Many report success with extractions with heated alcohols. Pull the cotton balls or plug from the neck and do the same. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. it's not rocket science. the hot plate set to med high. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Or you need to turn the Privacy Policy. Probably. Mix until paste. I have not taken the time this morning to reread Placebo's series of posts on this extraction The poster considers any it before use by heating in an oven or providone Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and 23) While draining boil a small amount of naptha about 5 ml Its important that we grind the mixture as fine patience! Beginners use /r/learningbees, Press J to jump to the feed. Many recommend long soak times, other short soak times.